This is the most versatile instrument in the CBC facility*, capable of a large number of experiments ranging from routine experiments to advanced multi-dimensional and multi-nuclear NMR as well as variable temperature (-90C to +90C). Advanced users must be comfortable with hardware manipulations in order to optimize the conditions and obtain high-quality data.
Specifications
Nickname:
- Sage
Frequency:
- 600 MHz
Temperature:
- -90 – +90 °C (183 – 363 K)
Probe:
- 5 mm “Smart” broadband probe (BBFO) with Z gradient
Software:
- Topspin 3.6 on a PC with Windows 10
Experimental
Sample Type:
- Solution
Nuclei:
- 1H, 13C
Availability
Access/Training:
- Pre-requisite – access and trained on the 40o-Cinnamon & need for advanced NMR experiments
- Request an appointment via FOM (Internal Users)
- Email Dan Conroy (External Users)
Time:
- Schedule via FOM; 2 hr. daytime limit (9am-8pm) and unlimited nights & weekends. Extended time is available for variable temperature experiments (by request).
Point of Contact
**UPDATE: A new probe has been purchased by the Department of Chemistry & Biochemistry for the 600-Sage. This probe is the newest generation of the Bruker iProbe. It will be a 5mm broadband (BBFO) probe with better performance and reliability than the current probe. The ETA for this probe is September 2023.
*For higher field instrumentation, please visit the CCIC Website. The 700 MHz in the Riffe building is equipped with a direct-detection 13C cryoprobe for ultra-high 13C sensitivity.